广西壮药材粪箕笃质量标准的研究.PDFVIP

第39 卷第1 期 Vol.39 No.1 井冈山大学学报( 自然科学版) 2018 年1 月 Jan. 2017 Journal of Jinggangshan University (Natural Science) 82 82 井冈山大学学报( 自然科学版) 文章编号：1674-8085(20 18)01-0082-05 广西壮药材粪箕笃 量标准的研究 * 庞丹清,魏中璇, 陈 勇,阙祖亮,魏江存,张 昕，庾延和 （广西中医药大学药学院，广西，南宁530200 ） 摘 要：目的 建立和完善广西壮药粪箕笃药材的质量标准。方法 根据 《中国药典》2015 年版第四部中药品标 准研究方法首次对粪箕笃药材进行水分、灰分、酸不溶灰分、浸出物及重金属的检测,并采用高效液相色谱法对 粪箕笃药材中千金藤 碱成分进行鉴定。结果 粪箕笃药材水分不高于 16.10%，总灰分不高于 13.90%，酸不溶 性灰分不高于 1.28%，浸出物不低于 9.29%，粪箕笃药材不含有千金藤 碱成分。结论 该方法可作为制定和完 善粪箕笃药材质量标准的依据。 关键词：壮药；粪箕笃；千金藤 碱；质量标准 中图分类号：R927.11 文献标识码：A DOI: 10.3969/j.issn.1674-8085.20 18.01.0 17 STUDY ON THE QUALITY STANDARD OF S TEPHANIA LONGA LOUR.FROM ZHUANG MEDICIME MATERIALS IN GUANGXI PANG Dan-qing, WEI Zhong-xuan, *CHEN Yong, QUE Zu-liang, WEI Jiang-cun, ZHANG Xin，YU Yan-he (College of Charmacy, Guangxi University of Chinese Medicine, Nanning, Guangxi 530200, China) Abstract Objective: To construct the quality standards of Stephania longa Lour. from Zhuang medicine materials in Guangxi. Methods: The characters as moisture, total ash, acid insoluble ash, extract and heavy metal of S. longa Lour. were detected based on pharmaceutical standard in 2015 version. Stepholidine in S. longa Lour. was determined by HPLC. Results: S. longa’s Lour. moisture, total ash, acid insoluble ash were not over 16.10%, 13.90% and 1.28% respectively, the extract was not less than 9.29%, and it had no Stepholidine. Conclusion: The results can be used as to develop and perfect the basis of S. longa Lour. quality standard ． Key words: Zhuang medicine; Stephania longa Lour.; stepholidine; quality standard 粪萁笃(Stephania longa Lour.)为防己科千金藤 [4]