有哪些信誉好的足球投注网站structure of methyl 1-oxo-3,5-diphenylcyclohexene-6-carboxylate结构的甲基1-oxo-3 5-diphenylcyclohexene-6-carboxylate.pdfVIP
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structure of methyl 1-oxo-3,5-diphenylcyclohexene-6-carboxylate结构的甲基1-oxo-3 5-diphenylcyclohexene-6-carboxylate
Synthesis of ({8[4,6Bis(bispyridin2ylmethylamino)[1,3,5]triazin... Molbank 2007, M557 /molbank/ Synthesis of ({8[4,6Bis(bispyridin2ylmethylamino)[1,3,5]triazine 2ylamino]octyl}—ethoxycarbonylmethylamino)acetic acid ethyl ester * Daniel Vomasta and Burkhard König Institute of Organic Chemistry, University of Regensburg, D93040 Regensburg, Germany * Author to whom correspondance should be addressed. Email: Burkhard.koenig@chemie.uniregensburg.de Keywords: Dipicolylamine, 2,4,6trischlorotriazine, iminodiacetic acid, twoprong Combination of recognition units in synthetic receptors typically increases binding constants, if cooperativity occurs.[1] Dipicolylamine (Dpa) biszinc complexes are known to bind phosphatedianions under physiological conditions with good affinities [2,3], whereas metal(II)iminodiacetate (M(II)IDA) complexes (metal(II) = copper(II), nickel(II) or zinc(II)) show affinity to Nterminal histidine.[2] Combining both units may lead to a selective binding of phosphorylated amino acid bearing Nterminal histidine. We report here a general synthetic route to ligands bearing a Dpa and an Ida site for metal ion complexation. The use of 6chloroN,N,N,N tetrakispyridin2ylmethyl[1,3,5]triazine2,4diamine ( ) in nucleophilic aromatic substitution provides a practical and versatile access to a variety of such twoprong Dpa receptors, [4] which is exemplarily shown on the preparation of compound 3. ({8[4,6Bis(b
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