使用NOVA软件，实现样品自动化进样与分析Autolab电化学工作站与瑞士万通灵快量化技术的结合.pdfVIP

Autolab 应用报告 自动化部分 /Applications/ 使用NOVA 软件实现样品自动化进样与分析Autolab 与瑞士万通灵快量化技术的结合 关键字： 样品处理器 自动样品处理 万通设备 自动滴定管 Sample processor; Automatic sample handling; Metrohm devices; Automatic burette Summary Automatic sample handling and analysis is very convenient for routine measurements on large number of samples. Beyond the obvious time benefit, automatic sample handling solutions also reduce the risk of errors and contamination and allow for unattended experiments. Metrohm offers a wide range of high performance liquid handling devices that can be directly controlled by the NOVA software. This allows for an easy integration of Metrohm devices with electrochemical measurements using Autolab instruments. This application note provides information on the combination of supported Metrohm device in the framework of a practical electrochemical measurement, performed with the NOVA software. 对于需要处理大量样品的日常分析，自动样品处理和分析是非常方便的，除了明显的节约时 间的优点外，自动样品处理还减少了污染的风险，，并且允许实验时无人值守。瑞士万通能 够提供多种高性能的液体处理设备，直接由NOVA 软件控制。这是Metrohm 设备与Autolab 电化学测试仪器的结合。本报告讲述了实际电化学测试中的这种结合。 支持的Metrohm 设备： NOVA 通过 USB 直接控制以下设备： 814, 815 and 858 样品处理器 846 加液器 而且，通过MSB 还可连接使用以下设备，例如： 800 Dosino 801 磁力搅拌器 803 滴定台 （磁力搅拌，吸排液功能） 最后，还有一些Metrohm 附件可以连接到上述设备： 786 摆头 802 螺旋搅拌器 823 隔膜泵 772 蠕动泵 所有控制设备需要的命令均在NOVA 软件Command 项下，Metrohm devices 内 All the commands related to the control of Metrohm devices can be found in the Metrohm devices group of commands (see Figure 1). Figure 1 – Metrohm devices are directly controlled by the NOVA software Experimental setup The example illustrated in this application note uses the following Metrohm devices: 800 Dosino with 20 ml burette 814 USB Sample Processor (1T/0P) 24 samples rack, single row (75 ml beakers) Two 823 membrane pumps The Dosino is connected to the sample processor through MSB. The sample processor is connected to the computer through USB. The two 82