舒心胶囊中虎杖提取工艺的研究.pdfVIP

舒心胶囊中虎杖提取工艺研究 于洛临张素中成冲(广东省中医研究所广州510095) 摘要：目的：研究舒心胶囊中虎杖最佳提取方法及提取．1：艺条fl：。方法：以UV、HPLC、薄层扫 描色谱法为手段，对比分析不同提取方法对虎杖总蒽醌含鼙及其相关成分的相对含量、虎杖营 含姑的影响，确立虎杖的提取方法：采川止交试验r考察加醇量、醇提时间、醇浓度3个影响 风素，以总葸醌、虎杖茁含量为综合评价指标，优选虎杖醇提最佳．I：艺条件。结果：虎杖单独 醇提为所得的虎杖苷含量较高，确立以虎杖单独醇提jI．艺：最佳提取．I：艺条什为8倍姑85％ 乙醇闸流提取2次，每次1．5小时。 关键词：虎杖：人黄素；虎杖苛；提取．r艺 of inShuxin onExtractionProcess cuspidatum Capsule Study Polygonum the extraction andthe Abstract：Objective：Tostudy optimum process optimum ionconditionof inShuxin extract polygonumcuspidatum to anal differentethanolextraction UV、TLC、HPLC，systematicysis process，resort of in different theeffectofthecontentthe componentpolygonumcuspidatumby extraction ethanolextraction the process，establish process：Adoptexperimentby theethanol magnitude、ethanol orthogonal，review contentofemodinand the withthe polydatin，establishoptimum time，appraise extractionof extraction processpolygonumcuspidatum．Results：Polygonumcuspidatum itselfhave themostcontentof ethanolextraction by got polydatin，establish isextraction ethanol；Theextraction process polygonumcuspidatumsingleby optimum is8timesamountof85％ethanolandcircumfluenceextraction2 conditioff times，1．5 hoursonetime．