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DOI:10.1002/celc.201500036Articles
Off-StoichiometryinAlluaudite-TypeSodiumIronSulfate
NaFe(SO)asanAdvancedSodiumBatteryCathode
2+2x2x43
Material
GosukeOyama,[a]Shin-ichiNishimura,[a,b]YuyaSuzuki,[a]MasashiOkubo,[a,b]and
AtsuoYamada*[a,b]
Analluaudite-typesodiumironsulfatehasrecentlybeendis-623Kproducetwostablephases:1)vanthoffite-structured
coveredasa3.8Vcathodematerialforlow-cost,high-power,NaFe(SO)and2)alluaudite-typeNaFe(SO)withacer-
6442+2x2x43
andefficientsodium-ionbatteries.Tooptimizethecomposi-tainnon-stoichiometry.Thepossiblecompositionalandstruc-
tionofthealluauditephaseandtoexplorefurthercom-turalflexibilitiesdemonstratedinthisworkinspirefurtherim-
pounds,wehavecarefullysurveyedtheNaSO-FeSObinaryprovementofthealluaudite-typesodiummetalsulfatesforad-
244
system.Solid-statereactionsatamoderatetemperatureofvancedsodium-ionbatteries.
1.Introduction
Large-scaleelectrochemicalenergystoragehasbeendemand-catesandphosphates,sulfatecompoundsgenerallyhavemore
edforitsuseinthepowergrid.Low-cost,high-power,andeffi-ionicMObonds,leadingtothehighoperatingpotential.[9]
cientbatteriescanload-le
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