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Materials Science and Engineering A 380 (2004) 402–407 Superplastic diffusion bonding of -TiAl-based alloy G.Q. Wu a,∗, Z. Huang a , C.Q. Chen a , Z.J. Ruan a , Y. Zhangb a School of Materials Science and Engineering, Beijing University of Aeronautics and Astronautics, Beijing 100083, China b State Key Laboratory for Advanced Metals and Materials, University of Science and Technology, Beijing 100083, China Received 6 June 2003; received in revised form 1 April 2004 Abstract With laser surface melting and conventional heat treatment, superplastic diffusion bonding of TiAl alloy samples was carried out. Three different microstructure, i.e. fully lamellar structure, fine dendritic structure and refined equiaxed structure are used and their effects on bonding quality were investigated, and the bond quality was assessed by shear test at room temperature. Sound bonds could be achieved at 900 ◦C by laser surface modification or by laser surface modification and pre-bond heat treatment at 1000 ◦C for 60 min, which is lower than conventional diffusion bonding temperature. The bonds were also post-bond heat treated at 1200 ◦C for 30 min, which improved the bond quality in all cases. The best shear strength of the bonds is greater than 80% of that of base metal. Keywords: TiAl-based alloy; Laser surface treatment; Superplastic diffusion bonding; Shear test 1. Introduction refined equiaxed structure are used in the bonding of TiAl alloys and their effects on bonding quality are investigated. Alloys based on the -TiAl intermetallic compound have been of much interest in recent years as light-weight, struc- tural materials for elevated tempera