有哪些信誉好的足球投注网站correlation of the rates of solvolysis of neopentyl chloroformate—a recommended protecting agent相关的溶剂分解率的新戊基chloroformate-a建议保护代理.pdfVIP
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correlation of the rates of solvolysis of neopentyl chloroformate—a recommended protecting agent相关的溶剂分解率的新戊基chloroformate-a建议保护代理
Int. J. Mol. Sci. 2011, 12, 1161-1174; doi:10.3390/ijm OPEN ACCESS International Journal of Molecular Sciences ISSN 1422-0067 /journal/ijms Article Correlation of the Rates of Solvolysis of Neopentyl Chloroformate—A Recommended Protecting Agent Malcolm J. D’Souza 1,*, Shannon E. Carter 1 and Dennis N. Kevill 2,* 1 Department of Chemistry, Wesley College, 120 N. State Street, Dover, DE 19901, USA 2 Department of Chemistry and Biochemistry, Northern Illinois University, DeKalb, IL 60115, USA * Authors to whom correspondence should be addressed; E-Mails: dsouzama@ (M.J.D.); dkevill@ (D.N.K.); Tel.: +1-302-736-2528 (M.J.D.); Fax: +1-302-736-2301 (M.J.D). Received: 6 January 2011; in revised form: 30 January 2011 / Accepted: 9 February 2011 / Published: 15 February 2011 Abstract: The specific rates of solvolysis of neopentyl chloroformate (1) have been determined in 21 pure and binary solvents at 45.0 °C. In most solvents the values are essentially identical to those for ethyl and n-propyl chloroformates. However, in aqueous-1,1,1,3,3,3-hexafluoro-2-propanol mixtures (HFIP) rich in fluoroalcohol, 1 solvolyses appreciably faster than the other two substrates. Linear free energy relationship (LFER) comparison of the specific rates of solvolysis of 1 with those for phenyl chloroformate and those for n-propyl chlor
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