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controllable layered structures in polyoxomolybdate-surfactant hybrid crystals可控的分层结构polyoxomolybdate-surfactant混合晶体
Materials 2010, 3, 158-164; doi:10.3390/ma3010158 OPEN ACCESS materials ISSN 1996-1944 /journal/materials Article Controllable Layered Structures in Polyoxomolybdate- Surfactant Hybrid Crystals Takeru Ito 1,2,* and Toshihiro Yamase 1,3,* 1 Chemical Resources Laboratory, Tokyo Institute of Technology, R1-21, 4259 Nagatsuta, Midori- ku, Yokohama 226–8503, Japan 2 Department of Chemistry, School of Science, Tokai University, 1117 Kitakaname, Hiratsuka 259–1292, Japan 3 (Inc.) MO Device, 2-14-10 Kanaiwa-higashi, Kanazawa 920–0335, Japan * Author to whom correspondence should be addressed; E-Mail: takeito@keyaki.cc.u-tokai.ac.jp (T.I.); yamase.modevice@ (T.Y.); Tel.: +81-463-58-1211 ex. 3737; Fax: +81-463-50-2094 (T.I.); Tel./Fax: +81-76-267-0468 (T.Y.) Received: 19 November 2009; in revised form: 23 December 2009 / Accepted: 4 January 2010 / Published: 6 January 2010 Abstract: Inorganic-organic hybrid crystals containing α-octamolybdate (Mo ) or 8 hexamolybdate (Mo6) were isolated by using hexadecyltrimethylammonium (C16) surfactant. The packing mode of the inorganic layers depended on a difference in the polyoxomolybdate molecular structure. The structure for both crystals consisted of alternate stacking of C16 organic bilayers and polyoxomolybdate inorganic layers with a periodicity of 24.4–24.6
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