biomass thermogravimetric analysis uncertainty determination methodology and sampling maps generation生物质热重量分析测定方法和不确定性抽样地图的一代.pdfVIP
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biomass thermogravimetric analysis uncertainty determination methodology and sampling maps generation生物质热重量分析测定方法和不确定性抽样地图的一代
Int. J. Mol. Sci. 2010, 11, 2701-2714; doi:10.3390/ijm OPEN ACCESS International Journal of Molecular Sciences ISSN 1422-0067 /journal/ijms Article Biomass Thermogravimetric Analysis: Uncertainty Determination Methodology and Sampling Maps Generation Jose A. Pazó 1, Enrique Granada 1,*, Ángeles Saavedra 2, Pablo Eguía 1 and Joaquín Collazo 1 1 ETS Ingenieros Industriales, University of Vigo, Lagoas-Marcosende s/n 36200–Vigo, Spain; E-Mails: jpazo@uvigo.es (J.A.P.); peguia@uvigo.es (P.E.) 2 ETS Ingeniería de Minas, University of Vigo. Lagoas-Marcosende s/n 36200–Vigo, Spain; E-Mail: saavedra@uvigo.es * Author to whom correspondence should be addressed; E-Mail: egranada@uvigo.es; Tel.: +34-986-812-183. Received: 3 June 2010; in revised form: 5 July 2010 / Accepted: 11 July 2010 / Published: 15 July 2010 Abstract: The objective of this study was to develop a methodology for the determination of the maximum sampling error and confidence intervals of thermal properties obtained from thermogravimetric analysis (TG), including moisture, volatile matter, fixed carbon and ash content. The sampling procedure of the TG analysis was of particular interest and was conducted with care. The results of the present study were compared to those of a prompt analysis, and a correlation between the mean values and maximum sampling errors of the methods were not observed. In general, low
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