template free synthesis of hollow ball-like nano-fe2o3 and its application to the detection of dimethyl methylphosphonate at room temperature免费模板合成中空球形nano-fe2o3及其应用在室温下methylphosphonate二甲酯的检测.pdfVIP
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template free synthesis of hollow ball-like nano-fe2o3 and its application to the detection of dimethyl methylphosphonate at room temperature免费模板合成中空球形nano-fe2o3及其应用在室温下methylphosphonate二甲酯的检测
Sensors 2012, 12, 4594-4604; doi:10.3390/s120404594 OPEN ACCESS sensors ISSN 1424-8220 /journal/sensors Article Template Free Synthesis of Hollow Ball-Like Nano-Fe O and 2 3 Its Application to the Detection of Dimethyl Methylphosphonate at Room Temperature Guokang Fan 1,2, You Wang 1, Meng Hu 1, Zhiyuan Luo 3, Kaihuan Zhang 1 and Guang Li 1,* 1 State Key Laboratory of Industrial Control Technology, Institute of Cyber Systems and Control, Zhejiang University, Hangzhou 310027, China; E-Mails: gkfan@ (G.F.); king_wy@ (Y.W.); vhumeng@126.com (M.H.); zhangkaihuan@ (K.Z.) 2 School of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China 3 Computer Learning Research Centre, Royal Holloway, University of London, Egham, Surrey TW20 0EX, UK; E-Mail: Zhiyuan.Luo@cs.rhul.ac.uk * Author to whom correspondence should be addressed; E-Mail: guangli@; Tel.: +86-571-8795-2268 ext. 8828. Received: 8 March 2012; in revised form: 29 March 2012 / Accepted: 30 March 2012 / Published: 10 April 2012 Abstract: This paper is focused on the template-free synthesis of nanosized ferric oxide (nano-Fe O ) and its application in quartz crystal microbalance (QCM) resonators to detect 2 3 dimethyl methylphosphonate (DMMP), a simulant of Sarin. The X-ray diffraction (XRD) patterns confirm that the synthesized samples are made of Fe O and the scanning electron
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