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Hollow TiO2 microspheres assembled with rutile mesocrystals Low-temperature one-pot synthesis and the photocatalytic performance》.pdf
Available online at CERAMICS INTERNATIONAL Ceramics International 41 (2015) 12317– 12322 /locate/ceramint Hollow TiO2 microspheres assembled with rutile mesocrystals: Low-temperature one-pot synthesis and the photocatalytic performance Lu-Lu Lai, Jin-Ming Wun State Key Laboratory of Silicon Materials and School of Materials Science and Engineering, Zhejiang University, Hangzhou 310027, PR China Received 9 May 2015; received in revised form 3 June 2015; accepted 13 June 2015 Available online 20 June 2015 Abstract Hollow TiO microspheres assembled with rutile mesocrystal nanorods were precipitated directly from a mixed aqueous solution of K TiO 2 2 (C O ) , H O and HNO at a low temperature of 80 1C. The hollow microspheres consisted of rutile mesocrystal nanorods with an average 2 4 2 2 2 3 diameter of 200 nm and length of 500 nm. The morphology evolution upon the reaction duration suggests that the microstructure is formed through a hydrolysis–dissolution–precipitation procedure. The unique nanostructure of the hollow microspheres showed remarkable ph
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