XRay Crystallography Facility OverviewKLB型X射线晶体学设施概述课件.pptVIP

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XRay Crystallography Facility OverviewKLB型X射线晶体学设施概述课件.ppt

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XRay Crystallography Facility OverviewKLB型X射线晶体学设施概述课件

Welcome! X-Ray Facility, 410-413 Kasha Laboratory Institute of Molecular Biophysics Florida State University Tallahassee, FL 32306-4380 /~xray X-Ray Facility Orientation History of the Facility Facility Resources Requirements Data Collection Data Processing Manuals Archiving Summary Contact Information History of the Facility-1 Core facility planned in 1990-92 Facility Director hired Feb 1993 Construction June – Sep 1993 Two generators Image Plate (IP) detector in January 1994 Elliott generator in 1995 History of the Facility-2 Cryo capabilities in 1996 Crystal chamber in 1999 Confocal mirror in Spring 2000 CCD w/ confocal mirror in Fall 2000 CryoCooler 700 w/ auto-refill in Fall 2000 Additional Linux machines in 2000 Complete renovation during 2002-03 Facility Resources Accessories Three Copper rotating anode generators Two automated area detectors Two confocal one total reflection mirrors Two cryo coolers One automated liquid Nitrogen refiller Linux and Windows NT computers Full time Faculty/Staff (State-line) Resources-1 Generators Two Rigaku H2R 5.4 kW generators One Elliott GX-30 3.0 kW generator Area detector-1 (IP) R-Axis IIc (1994) w/ confocal blue mirror 65-450 mm sample-detector distance 0-25 degree non-zero 2-theta capability Oxford Cryostream 600 cold head Resources-2 Area detector-2 (CCD) Mar165 CCD w/ confocal purple mirror 35-380 mm sample-CCD distance Limited non-zero 2-theta capability Oxford Cryostream 700 cold head Long short Supper (total-reflection) mirrors Stand-alone IP Bio Unit I Analytical Lab Accessories-1 Leica stereo microscope w/ Moticam digital camera Nikon Optiphot microscope w/ analog camera Stereo zoom microscopes DVD-R +R writers DDS-3 -4 tape drives FireWire (Maxtor: 60 80 GB) drives Windows NT and five Linux computers Accessories-2 Cold room for 4°C crystallization set-up Room for ambient crystallization set-up Crystallization chamber Temperature humidity monitoring Dry Cryo Shipper Long-term sample stora