synthesis of molecularly imprinted polymers for amino acid derivates by using different functional monomers分子印迹聚合物的合成氨基酸衍生物通过使用不同功能单体.pdfVIP

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synthesis of molecularly imprinted polymers for amino acid derivates by using different functional monomers分子印迹聚合物的合成氨基酸衍生物通过使用不同功能单体.pdf

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synthesis of molecularly imprinted polymers for amino acid derivates by using different functional monomers分子印迹聚合物的合成氨基酸衍生物通过使用不同功能单体

Int. J. Mol. Sci. 2011, 12, 1735-1743; doi:10.3390/ijm OPEN ACCESS International Journal of Molecular Sciences ISSN 1422-0067 /journal/ijms Article Synthesis of Molecularly Imprinted Polymers for Amino Acid Derivates by Using Different Functional Monomers Sonia Scorrano *, Lucia Mergola, Roberta Del Sole and Giuseppe Vasapollo * Dipartimento di Ingegneria dell’Innovazione,Universitàdel Salento, via per Arnesano Km 1, 73100 Lecce, Italy; E-Mails: lucia.mergola@unisalento.it (L.M); roberta.delsole@unisalento.it (R.D.S.) * Authors to whom correspondence should be addressed; E-Mails: sonia.scorrano@unisalento.it (S.S.); giuseppe.vasapollo@unisalento.it (G.V.); Tel.: +39-0832-297265; Fax: +39-0832-297268. Received: 14 January 2011; in revisedform: 1 February 2011 / Accepted: 1 March 2011 / Published: 7 March 2011 Abstract: Fmoc-3-nitrotyrosine (Fmoc-3-NT) molecularly imprinted polymers (MIPs) were synthesized to understand the influence of several functional monomers on the efficiency of the molecular imprinting process. Acidic, neutral and basic functional monomers, such as acrylic acid (AA), methacrylic acid (MAA), methacrylamide (MAM), 2-vinylpyridine (2-VP), 4-vinylpyridine (4-VP), have been used to synthesize five different polymers. In this study, the MIPs were tested in batch experiments by UV-visible spectroscopy in order to evaluate their binding properties. The MIP prepared with 2-VP