毛细管电泳法分离丹参水溶性有效成分-天津中草药杂志社.PDF

　Chinese Traditional and Herbal Drugs　2000 31 5 ·337· —— 、 ( 1160 11)　　芮建中 　邹汉法 　　　　　　　　　　　　　　　　袁倚盛　 凌树森 　　( DSS)、( PA H)( PA)。 ( )、 、、 CT AB p H 、,、、, : 7. 0, 0. 5 / , 200 / 20 ∶5 pH m mol L CTAB mmol L , 75 μm(id )× 34. 5 ( eff. 30) m ( 20℃), 10 kV ( 6 s), 8 。 8 20% -,( , - ) , 、 kV min p HBA DSS PA H PA , 40 /。 　　　　 Separation of Water-Soluble Active Principles of Danshen (Salvia miltiorrhiza ) , Danshensu Protocatechuic Aldehyde and Protocatechuic Acid by HPCE 　　National Ch romatographi Resear h Analysis Centre, Dalian Institute of Ch emi al Physi s, Chinese A ademy of S ien es ( Dalian 116011)　 Rui Jianzhong and Zou Hanfa 　　Department of Clini al Pharma ology, Jinling Hospital　Yuan Yisheng and Lin Shusen 　 　 - . — ( ) , Abstract Water soluble a tive prin iples of Sal via milt ior rh iz e Bge Danshensu DSS ( ) ( ) . proto ate hui aldehy de PA H and proto ate hui a id PA w ere separated by HPCE M any fa tors that , , an affe t the resolution sensitivity and olumn effi ien y of organi anion in luding the on entration of etyltrimethyl ammonium bromide ( CTAB) , p H value, on entration of phosphate buffer, per entage of organi modifier in the buffer , running voltage,