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Synthesis of Fan-Shaped C3 Molecule with Three Glycyrrhetinic Acid Units and Self-Assembly Properties.pdf
FULLPAPER
SynthesisofFan·ShapedC3MoleculewithThreeGIycyrrhetinic
AcidUnitsandSelf-AssemblyProperties
Hu，Jun(胡君) Yu，Libing(于立冰) Zhang，Meng(章萌) Ju，Yong 。(巨勇)
KeyLaboratoryofBioorganicPhosphorusChemistry ＆ChemicalBiology(MinistryofEducation)，Departmentof
Chemistry，TsinghuaUniversity，Beijing100084，China
StateKeyLaboratoryofAppliedOrganicChemistry，LanzhouUniversity，Lanzhou，Gansu730000，China
A novelfan—shapedC3moleculewiththreeglycyrrhetinicacidunitswassynthesizedvia “clickchemistry’’in
highyieldnadhteself-assemblycharacteristicswerestudiedindifferentmixedsolvents．
Keywords terpenoids，C3molecules，self-assembly
Introduction
MeO2
Symmetryplaysan importantrole in thechemical
topics such as chemical selectivity, supramolecular
self-assembly，chiralrecognition，asymmetric synthesis
and catalysis．’ Among various symmetric organic
compounds，versatileand available C3moleculesrae
widely used in organicnanotubes，redox active chro—
mophoresand controlled self-assembly．。一 Asarepre—
sentativeofC3molecules．1．3．5．triazineiswell-known
inorgna icchemistryandisusedinavarietyofapplica—
tionsas2，4，6一mono一，di—ortrisubstituted derivatives o N＼丫o
endowedwithdifferentsubstituents．’ Duetothehigh N N
reactivity of chlorine atoms in cyanuric chloride
(2，4，6一trichloro．1，3，5一rtiazine)towradnucleophiles，itis
generallyusedasthestartingmaterialfortheprepraa— Me
tion ofdifferenttriazinederivatives，“including den—
drimersinwhichthetriazineringactsastheconstruc—
tivecOre．2-5 一
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