gacl3催化氢化胺化胍化反应以及一系列钛配合物合成及表征-gac l3 catalyzes the amination of guanidine and synthesis and characterization of a series of titanium complexes.docxVIP

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gacl3催化氢化胺化胍化反应以及一系列钛配合物合成及表征-gac l3 catalyzes the amination of guanidine and synthesis and characterization of a series of titanium complexes.docx

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gacl3催化氢化胺化胍化反应以及一系列钛配合物合成及表征-gac l3 catalyzes the amination of guanidine and synthesis and characterization of a series of titanium complexes

目录第一章绪论·················································································11.1引言·····················································································11.2炔烃的分子间氢化胺化的研究进展···············································11.3 胺的胍化的研究进展·······························································121.4 本论文的研究目的和意义·························································18参考文献···················································································18第二章GaCl3催化的炔烃的分子间氢化胺化反应·····································222.1引言····················································································222.2结果与讨论···········································································222.2.1反应条件的优化·····························································222.2.2底物拓展······································································252.2.3 反应机理的DFT研究262.3结论····················································································302.4实验操作··············································································302.4.1 仪器和药品···································································302.4.2GaCl3 催化的氢化胺化的反应步骤302.5 化合物表征数据·····································································31参考文献···················································································37第三章GaCl3催化的胺与碳二亚胺的加成：胺的胍化·······························423.1引言·····················································································423.2结果与讨论···········································································423.2.1反应条件的优化·····························································423.2.2底物拓展······································································433.2.3机理研究······································································463.3结论····················································································473.4实验操作········································································

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gacl3催化氢化胺化胍化反应以及一系列钛配合物合成及表征-gac l3 catalyzes the amination of guanidine and synthesis and characterization of a series of titanium complexes.docxVIP