微波水热法制备CdS球形团簇-IngentaConnect.PDF

1652 2012 40 11 Vol. 40 No. 11 2 0 1 2 1 1 JOURNAL OF THE CHINESE CERAMIC SOCIETY November 2012 CdS 1 1 2 1 1 1 (1. 710021 2. 201804) [Cd(CH COO) 2H O](Na S O 5H O)CdS 3 2 · 2 2 2 3 · 2 n(S)/n(Cd)()CdS Cd(CH COO) 2H O 3 2 · 2 – CdS CH COO 3 n(S)/n(Cd)CdS UV–Vis CdS TQ132.4+4 A 0454–5648(2012)11–1652–08 2012–10–31 10:54:55 /kcms/detail/11.2310.TQ1054.201211.1655_019.html Synthesis of Sphere-Like CdS Cluster-shaped Structure by Microwave Hydrothermal Process ZHANG Qinfeng1 1 2 1 1 1 HUANG Jianfeng HU Baoyun CAO Liyun ZHANG Yongliang WU Jianpeng (1. Key Laboratory of Auxiliary Chemistry Technology for Light Chemical Industry, Ministry of Education, Shaanxi University of Science Technology, Xian 710021, China; 2. School of Material Science and Engineering, Tongji University, Shanghai 201804, China) Abstract: CdS microcrystalline with a sphere-like cluster-shaped structure was prepared with cadmium acetate (Cd(CH3COO)2 ·2H2O) and sodium thiosulfate (Na S O ) as raw materials by a microwave hydrothermal process. The influences of microwave hydrothermal