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synthesis and properties of poly(isothianaphthene methine)s with chiral alkyl chain合成和性能的聚(isothianaphthene次甲基)与手性烷基链
Materials 2012, 5, 317-326; doi:10.3390/ma5020317 OPEN ACCESS materials ISSN 1996-1944 /journal/materials Article Synthesis and Properties of Poly(Isothianaphthene Methine)s with Chiral Alkyl Chain 1 1 2 1 Yu Innami , Hirotsugu Kawashima , Rafaël H. L. Kiebooms , Hideaki Aizawa , Kiyoto Matsuishi 1 and Hiromasa Goto 1,* 1 Institute of Materials Science, Graduate School of Pure and Applied Sciences, University of Tsukuba, Tsukuba, Ibaraki 305-8573, Japan; E-Mails: s-yinnami@ims.tsukuba.ac.jp (Y.I.); s-hkawashima@ims.tsukuba.ac.jp (H.K.); aizawa@bunko2.bk.tsukuba.ac.jp (H.A.); kiyoto@bk.tsukuba.ac.jp (K.M.) 2 European Patent Office, Patentlaan 3-9, 2288 EE The Hague, The Netherlands; E-Mail: rkiebooms@ * Author to whom correspondence should be addressed; E-Mail: gotoh@ims.tsukuba.ac.jp; Tel.: +81-29-853-5128; Fax: +81-29-853-4490. Received: 29 December 2011; in revised form: 21 January 2012 / Accepted: 6 February 2012 / Published: 16 February 2012 Abstract: We synthesized poly(isothianaphthene methine)s with chiral alkyl chains in the substituent. Resultant polymers are soluble in THF and CHCl . Structure of the polymers 3 was characterized with FT-IR, FT-Raman, and UV-Vis-NIR optical absorption spectroscopy. They showed low-bandgap both in solution and in a form of film. Optical activity of the polymers was confirmed with optical rotatory dispersion. Dop
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