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QUALITY CONTROL PROCEDURES FOR (质量控制程序)
QUALITY CONTROL PROCEDURES FOR PESTICIDE RESIDUES ANALYSIS Guidelines for Residues Monitoring in the European Union Third Edition 2003 Document No. SANCO/10476/2003 2003-08-27 Prepared on behalf of the European Commission by Stewart Reynolds (UK) and the Scientific Advisory Committee, following discussions at the 3rd EU Workshop on Co-ordinated Analytical Quality Control, York, UK, 5 - 6 June 2003 QUALITY CONTROL PROCEDURES FOR PESTICIDE RESIDUES ANALYSIS ?Error!Marcador no definido. Introduction ?Error!Marcador no definido. Accreditation ?Error!Marcador no definido. Sampling, transport, processing and storage of samples ?Error!Marcador no definido. Sampling ?Error!Marcador no definido. Laboratory sample transportation ?Error!Marcador no definido. Sample preparation and processing prior to analysis ?Error!Marcador no definido. Pesticide standards, calibration solutions, etc. ?Error!Marcador no definido. Identity and purity of standards ?Error!Marcador no definido. Preparation and storage of stock standards ?Error!Marcador no definido. Preparation, use and storage of working standards ?Error!Marcador no definido. Testing and replacement of standards ?Error!Marcador no definido. Extraction and concentration ?Error!Marcador no definido. Extraction conditions and efficiency ?Error!Marcador no definido. Extract concentration and dilution to volume ?Error!Marcador no definido. Contamination and interference ?Error!Marcador no definido. Contamination ?Error!Marcador no definido. Interference ?Error!Marcador no definido. Analytical calibration, representative analytes, matrix effects and chromatographic integration ?Error!Marcador no definido. General requirements ?Error!Marcador no definido. Calibration ?Error!Marcador no definido. Representative analytes ?Error!Marcador no definido. Matrix effects and matrix-matched calibration ?Error!Marcador no definido. Standard Addition ?Error!Marcador no definido. Effects of pesticide mixtures on calibration ?Error!Marcador no
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